Column: NanoChrom BP-624
Dimension: 30m × 0.32mm × 1.80um
Carrier: Hydrogen, flow 2.3 mL/min
Inlet: Split, 260 °C, split column flow: 60 mL/min
Oven: 40 °C (hold 20min) to 240 °C (hold 20min) at 10 °C /min
Sample: USP class 1 residual solvent mixture
Detector: FID 280 °C