GC: Shimadzu GC-2030
Cat no: NanoChrom BP-1701MS 30m × 0.25mm × 0.25um
Oven: 60 °C (0.3 min) , 60 °C/min to 170 °C, 10 °C/min to 215 °C (12 min) , 1 °C/min to 240 °C
(12 min) , 30 °C/min to 280 °C (5 min) ,
Carrier: Nitrogen, constant flow 0.7 mL/min
Inlet: Split, 220 °C.
Detector: ECD 300 °C