Column: NanoChrom BP-50+MS
Dimension: 30m × 0.32mm × 0.25um
Carrier: Nitrogen, split column flow: 1.5 mL/min
Inlet: Split, 270 °C, split ratio: 20: 1
Oven: 100 °C (hold 2 min) to 250 °C at 10 °C/min
Inject Volume: 1 uL
Solvent: 二氯甲烷
Detector: FID 280 °C