Column: NanoChrom BP-5MS
Dimension: 30m × 0.25mm × 0.25um
Carrier: Hydrogen, constant flow 1.5 mL/min
Inlet: Split, 275 °C, split ratio: 60: 1
Oven: 50 °C (hold 0.5 min.) to 150 °C (hold 8 min ) at 20°C/min to 230 °C (hold 20 min ) at
20°C/min to 260 °C (hold 5 min )
Inject Volume: 偶氮染料 1 uL
Detector: FID 325 °C