Analysis Method

Product Specification

Product Result

Chemical Purity by HPLC/UV

≥98%

99.95%

Identity by ¹H NMR

Conforms to Structure

Pass

Identity by ¹³C NMR

Conforms to Structure

Pass

Identity by Mass Spectrometry

Conforms to Structure

Pass

Isotope Incorporation by Mass Spectrometry

≥90% D/Molecule

93.14%D/Molecule

Intended Use

This material is intended only for laboratory use in analytical and R+D applications. It not suitable for human/animal consumption or for household use.

Hazards

Read Material Safety Data Sheet (MSDS) and understand any potential hazard(s) prior to the use of this product. All chemicals should be considered potentially hazardous in nature and should only be handled by qualified personnel using established good laboratory practices.

Instrument:

Shimadzu LC-20AD

Column:

Eclipse XDB C₁₈ 4.6×250 mm, 5 μm

Mobile Phase:

A: Water   B: Acetonitrile

Gradient:

A:B(40:60) ，maintain to 21min 

Flow Rate:

1.5 mL/min from 1 min to 10 min

2.0 mL/min from 10 min to 20 min

1.5 mL/min from 20 min to 21 min

Wavelength:

279nm

Acquisition Date:

Jul 8^th, 2019

Peak #

Ret. Time (min.)

Area (mAU)

Height (mAU)

Area %

1

 1.811

 5383

 1204

 0.037

2

 3.544

 2182

 311

 0.015

3

 8.956

 14643560

 1083460

 99.948

Total

 14651126

 1084975

100.000

Instrument:

Bruker ANANCE 300MHz

Solvent:

CDCl₃

Acquisition Date:

Jul 5^th, 2019